Lab Reports

Scientific Analysis Laboratories
CERTIFICATE OF ANALYSIS
| Report Number: |
1610083 |
| Date of Report: |
14th July 2009 |
| Client: |
Pillbox 38 (UK) Ltd Suite 3a Brookmill Complex Branch Road Lower Darwen Lancashire BB3 0PR |
| Client Contact: |
Mr Jason Cropper |
| Client Job Reference: |
Totally Wicked Esmoking Liquid |
| Date Job Received at SAL: |
01April2009 |
| Date Analysis Started: |
07April2009 |
The results reported relate to samples received at the laboratory
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation
This report should not be reproduced except in full without the written approval of the laboratory
Tests covered by this certificate were conducted in accordance with SAL SOPs
Key to symbols used in this report:
W: Analysis was performed at another SAL laboratory
S: Analysis was subcontracted
N: Analysis is not UKAS accredited
U: Analysis is UKAS accredited
Report written by: nbsp; C. Rodger
Laboratory Manager
Report checked R. Hare
and authorised by: Laboratory Manager (Air Division)
Analysis of the Content of Totally Wicked ESmoking
Liquid supplied by Pill Box 38 (UK) Ltd
A sample of Totally Wicked ESmoking Liquid was supplied to Scientific Analysis Laboratories Limited, to determine the percentage level of nicotine it contained and other compounds present. The sample was analysed by Gas Chromatography – Mass Spectrometry.
The sample supplied was a 30ml bottle of 36mg Super High eliquid.
The Nicotine level was found to be : 1.8% (w/w).
The following pages of this report, give a more detailed breakdown of the analysis and details of other
compounds found.
Note: On the following pages the term “LOD” means Limit of Detection, this is the lowest amount of a sample that can be
detected using the technique GC/MS (Gas Chromatography Mass
Spectrometry).
Supplement to Report Number: 1610083
Client Job Reference:
|
SAL Ref: |
161008 001 |
| Client Ref: |
Pillbox 38 (UK) Ltd |
| Type: |
Oil |
| Ingredients |
Method |
Units |
LOD |
Symbol |
|
| Tobacco essencial |
n/a |
% |
n/a |
N |
<5% |
| Tobacco leaf oil |
n/a |
% |
n/a |
N |
<5% |
| Nicotine (from tobacco leaf) |
n/a |
% |
n/a |
N |
<3% |
| 2,3,5Trimethylpyrazine |
n/a |
% |
n/a |
N |
<1% |
| 2,3,5,6Tetramethylpyrazine |
n/a |
% |
n/a |
N |
<1% |
| 2,5Dimethylpyrazine |
n/a |
% |
n/a |
N |
<1% |
| 2Acetypyrazine |
n/a |
% |
n/a |
N |
<1% |
| 2Methyl butyric acid |
n/a |
% |
n/a |
N |
<1% |
| Terp ineol |
n/a |
% |
n/a |
N |
<1% |
| Ethyl maltol |
n/a |
% |
n/a |
N |
<1% |
| Guaiacol |
n/a |
% |
n/a |
N |
<1% |
| Acetyl pyridine |
n/a |
% |
n/a |
N |
<2% |
| Octalactone (gamma) |
n/a |
% |
n/a |
N |
<1% |
| Pure water |
n/a |
% |
n/a |
N |
<10% |
| Propylene Glycol |
n/a |
% |
n/a |
N |
<65% |
| Glycerol |
n/a |
% |
n/a |
N |
<20% |
Totally Wicked ESmoking Liquid
Supplement to Report Number: 1610083
Client Job Reference:
| SAL Ref: |
161008 001 |
| Client Ref: |
Pillbox 38 (UK) Ltd |
| Type: |
Oil |
| Semi Volatile Organic Compounds Screen |
Method |
Units |
LOD |
Symbol |
|
| Nicotine |
GC/MS |
% |
0.001 |
N |
1.8 |
| |
| Triethylene Glycol* |
GC/MS |
% |
0.001 |
N |
0.055 |
| Tetraethylene Glycol* |
GC/MS |
% |
0.001 |
N |
0.078 |
| Pentaethylene |
GC/MS |
% |
0.001 |
N |
0.040 |
This sample was analysed using an Agilent 6890 GC5973 MSD operated in scanning mode from 35450 m/z.
Compounds detected were subjected to a library search with results confirmed by the operator.
*Results are semi quantitative